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Mechanical ASTM E45


Standard Test Methods for Determining the Inclusion Content of Steel

These test methods cover a number of recognized procedures for determining the nonmetallic inclusion content of wrought steel. Macroscopic methods include macroetch, fracture, step-down, and magnetic particle tests. Microscopic methods include five generally accepted systems of examination. In these microscopic methods, inclusions are assigned to a category based on similarities in morphology, and not necessarily on their chemical identity. Metallographic techniques that allow simple differentiation between morphologically similar inclusions are briefly discussed. While the methods are primarily intended for rating inclusions, constituents such as carbides, nitrides, carbonitrides, borides, and intermetallic phases may be rated using some of the microscopic methods. In some cases, alloys other than steels may be rated using one or more of these methods; the methods will be described in terms of their use on steels.

This practice covers procedures to perform JK-type inclusion ratings using automatic image analysis in accordance with microscopic methods A and D. Depending on the type of steel and the properties required; either a macroscopic or a microscopic method for determining the inclusion content or combination of the two methods, may be found most satisfactory. These test methods deal only with recommended test methods and nothing in them should be constructed as defining or establishing limits of acceptability for any grade of steel.

Significance and Use

These test methods cover four macroscopic and five microscopic test methods (manual and image analysis) for describing the inclusion content of steel and procedures for expressing test results. Inclusions are characterized by size, shape, concentration, and distribution rather than chemical composition. Although compositions are not identified, Microscopic methods place inclusions into one of several composition-related categories (sulfides, oxides, and silicates – the last as a type of oxide).

The macroscopic test methods evaluate larger surface areas than microscopic test methods and because examination is visual or at low magnifications, these methods are best suited for detecting larger inclusions. Macroscopic methods are not suitable for detecting inclusions smaller than about 0.40 mm (1/64 in.) in length and the methods do not discriminate inclusions by type.

The microscopic test methods are employed to characterize inclusions that form as a result of deoxidation or due to limited solubility in solid steel (indigenous inclusions). These inclusions are characterized by morphological type, that is, by size, shape, concentration, and distribution, but not specifically by composition. The microscopic methods are not intended for assessing the content of exogenous inclusions (those from entrapped slag or refractories).

Because the inclusion population within a given lot of steel varies with position, the lot of steel varies with position; the lot must be statistically sampled in order to assess its inclusion content. The degree of sampling must be adequate for the lot size and its specific characteristics. Materials with very low inclusion contents may be more accurately rated by automatic image analysis, which permits more precise microscopic ratings.

Results of macroscopic and microscopic test methods may be used to qualify material for shipment, but these test methods do not provide guidelines for acceptance or rejection purposes. Qualification criteria for assessing the data developed by these methods can be found in ASTM product standards or may be described by purchaser-producer agreements. By agreements between producer and purchaser, this practice may be modified to count only certain inclusion types and thicknesses, or only those inclusions above a certain severity level, or both. Also, by agreement, qualitative practices may be used where only the highest severity ratings for each inclusion type and thickness are defined or the number of fields containing these highest severity ratings are tabulated.

These test methods are intended for use on wrought metallic structures. While a minimum level of deformation is not specified, the test methods are not suitable for use on cast structures or on lightly worked structures. Guidelines are provided to rate inclusions in steels treated with rare earth additions or calcium-bearing compounds. When such steels are evaluated, the test report should describe the nature of the inclusions rated according to each inclusion category (A, B, C, D).

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Extracted with permission, from ASTM Standard E-45-05e1, 2007, “Standard Test Methods for Determining the Inclusion Content of Steel,” copyright ASTM International, 100 Barr Harbor Drive, West Conshohocken, PA 19428. A copy of the complete standard may be purchased from ASTM International, www.astm.org.